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X-ray Absorption Near Edge Structure spectroscopy

Subcategory: spectroscopic
Standard reference: Fleet, M. E. (2005), Prietzel et al. (2011)
Papers: 2 | Mentions: 3

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Description

Sulfur K-edge X-ray Absorption Near Edge Structure spectroscopy was used to determine sulfur speciation in solid samples including bedrock, soils, and sediments. Linear combination fitting was used to quantify different sulfur forms including pyrite, elemental sulfur, sulfate, and organic sulfur.

Typical Equipment

  • synchrotron X-ray sources
  • XANES spectroscopy equipment
  • ATHENA software for data analysis

Output Measurements

  • sulfur speciation percentages
  • elemental sulfur content
  • pyrite content
  • organic sulfur content

Papers Using This Protocol (2)

article

Sulfur Biogeochemical Cycling and Redox Dynamics in a Shale-Dominated Mountainous Watershed

2022Journal of Geophysical Research: Biogeosciencesusing
article

Porewater Lead Concentrations Limited by Particulate Organic Matter Coupled With Ephemeral Iron(III) and Sulfide Phases during Redox Cycles Within Contaminated Floodplain Soils

2021Environmental Science & Technologyusing